IOTA Dimethiconol. Herein, R1, R2 and R3 are as defined above, and R4 is each independently hydrogen or a substituted or unsubstituted monovalent hydrocarbon group, preferably C1-C4 alkyl. A powder foundation was prepared by step A of grinding and mixing ingredients 1 to 9 until uniform, step B of mixing ingredients 11 to 14 until uniform, adding the mix to A and mixing until uniform, step C of adding ingredient 10 to B, and step D of press molding C in a mold. The silicone resin of 1 or 2 wherein in formula (1), a is a number of 0.01 to 0.2. A W/O blusher was prepared by step A of mixing ingredients 1 to 7 while heating, step B of mixing ingredients 8 to 10 and 12 until uniform, step C of mixing A and B, step D of mixing ingredients 11 and 13, and step E of slowly adding D to C while stirring, and emulsifying. The hydrolytic condensation is conducted preferably under acidic conditions and more preferably an acidic substance is added as the catalyst. The label of the cosmetic ingredient list has the following rules: 1 The names of the ingredients identified are in the order of their content in the formula, ie the higher the ranking, the higher the content of this ingredient in the cosmetic. The cosmetic composition of any one of 9 to 16, further comprising a UV absorbing agent or UV absorbing/scattering agent. The solution was heated at 130° C. to remove the ethanol formed and excess of water, after which it was cooled. Tested, Effective, Affordable Silicone manufacturers voluntarily support health and environmental testing to provide greater scientific understanding of silicone materials used in consumer and industrial applications. Blend of PEG, PPG-18, 18 Dimethicone. At the end of dropwise addition, the solution was heated at 40-60° C. for 5 hours to conduct hydrolytic condensation reaction, yielding a silicone resin solution. A film of this silicone resin had a refractive index of 1.501. The solution was heated at 100° C. for 3 hours, then at 130° C. for 2 hours to remove the ethanol formed and excess of water, after which it was cooled. 8. Exemplary inorganic salts include sodium, potassium, magnesium, calcium, aluminum, zirconium and zinc salts of inorganic acids such as hydrochloric acid, sulfuric acid, carbonic acid, and nitric acid. It is preferred that a crosslinked organopolysiloxane polymer be swollen with a liquid oil by incorporating the liquid oil in an amount of more than its own weight. A film of this silicone resin had a refractive index of 1.503. In the prior art, silicone resins are widely used as cosmetic ingredients in make-up cosmetics (e.g., foundations, lipsticks, eye shadows and mascaras), UV care cosmetics, and hair care cosmetics because of their film-forming ability, water resistance, sweat resistance and sebum resistance. Also firmness of a lipstick can be improved by adding Silicone Resin without impacting negatively the pay out and reducing the tendency to break from the mold. Also included are naturally occurring polymers such as cellulose and derivatives thereof, keratin, collagen and derivatives thereof. Exemplary amine salts and amino acid salts include salts of amines such as triethanolamine, and salts of amino acids such as glutamic acid. The subscript e is a number of 0 to 0.6. Examples of the linear acrylic-silicone copolymer include KP-541, KP-543, KP-545, KP-549, KP-550, KP-545L, KP-561P, KP-562P, KP-575, and KP-578 from Shin-Etsu Chemical Co., Ltd. If c is more than 0.2, the film becomes hard and brittle. Or silicones, I should say—because these slippery ingredients go under dozens of different names, with new compounds being developed all the time.. That makes them hard to identify and even harder to avoid, as they've become the new normal in beauty formulations, from makeup to skincare to haircare. The cosmetic composition of 13 wherein the crosslinked organopolysiloxane polymer is a crosslinked organopolysiloxane polymer having a polyether or polyglycerol group. If triphenylsilanol is added in step (B-i), side reaction with M units takes place to form a by-product (C6H5)3SiO—SiR13. *1 KF-6105 by Shin-Etsu Chemical Co., Ltd. Branched polyglycerol-modified silicone *3, Branched polyglycerol-modified silicone *4, Acrylamide/acryloyldimethyltaurine Na copolymer *5, Dimethyltaurineammonium acrylate/VP copolymer *6. A panel of 50 professional female members evaluated the lipstick with respect to spread upon application, stickiness, color irregularity upon finishing, lasting quality (retention, as evaluated after 8 hours from application) in accordance with the same method as used for the evaluation of the emulsion type cream foundation. A mascara was prepared by step A of adding ingredients 7 and 13 to ingredient 9 and mixing the contents uniformly while heating, step B of adding ingredients 1 to 6 and 8 to A and mixing the contents uniformly, step C of adding ingredients 10, 11 and 12 to B, and uniformly dispersing the contents on a roller. Common Molding Clay; Carved Molding Clay; Support. Suitable acidic substances include hydrochloric acid, sulfuric acid, p-toluenesulfonic acid, methanesulfonic acid, trifluoromethanesulfonic acid, phosphoric acid, acetic acid and citric acid while they may be used alone or in admixture. The cream on the quartz plate was immersed in water for 40 minutes, after which transmittance was measured again. FREE Shipping on orders over $25 shipped by Amazon. Suitable oil-soluble gelling agents include metal soaps such as aluminum stearate, magnesium stearate, and zinc myristate; amino acid derivatives such as N-lauroyl-L-glutamic acid and α,γ-di-n-butylamine; dextrin fatty acid esters such as dextrin palmitate, dextrin stearate, and dextrin 2-ethylhexanoate palmitate; sucrose fatty acid esters such as sucrose palmitate and sucrose stearate; fructooligosaccharide fatty acid esters such as fructooligosaccharide stearate and fructooligosaccharide 2-ethylhexanoate; benzylidene derivatives of sorbitol such as monobenzylidene sorbitol and dibenzylidene sorbitol; and organo-modified clay minerals such as dimethylbenzyldodecylammonium montmorillonite clay and dimethyldioctadecylammonium montmorillonite clay. A reactor was charged with 70 g of hexamethyldisiloxane, 210 g of triethoxyphenylsilane, 100 g of ethyl polysilicate having a SiO2 content of 40%, and 110 g of IPA. The silicone resin of Comparative Example 1 was a high viscosity liquid. Examples of the silicone oil used herein include linear or branched organopolysiloxanes ranging from low viscosity to high viscosity such as dimethylpolysiloxane, tristrimethylsiloxymethylsilane, caprylylmethicone, phenyltrimethicone, tetrakistrimethylsiloxysilane, methylphenylpolysiloxane, methylhexylpolysiloxane, methylhydrogenpolysiloxane, and dimethylsiloxane-methylphenylsiloxane copolymers; cyclic organopolysiloxanes such as octamethylcyclotetrasiloxane, decamethylcyclopentasiloxane, dodecamethylcyclohexasiloxane, tetramethyltetrahydrogencyclotetrasiloxane, and tetramethyltetraphenylcyclotetrasiloxane; silicone rubbers such as amino-modified organopolysiloxane, pyrrolidone-modified organopolysiloxane, pyrrolidone carboxylic acid-modified organopolysiloxane, gum-like dimethylpolysiloxane having a high degree of polymerization, gum-like amino-modified organopolysiloxane, gum-like dimethylsiloxane-methylphenylsiloxane copolymers; and silicone gum, silicone gum in cyclic organopolysiloxane, higher alkoxy-modified silicone (e.g., stearoxysilicone), higher fatty acid-modified silicone, alkyl-modified silicone, long chain alkyl-modified silicone, amino acid-modified silicone, fluorine-modified silicone. IOTA 203 Methyl Low Hydrogen Silicone Oil . The cosmetic composition of any one of 9 to 15, further comprising a powder. Exemplary surfactants include KSG-210, 240, 310, 320, 330, 340, 320Z, 350Z, 710, 810, 820, 830, 840, 820Z, 850Z, KF-6011, 6013, 6043, 6028, 6038, 6048, 6100, 6104, 6105, 6106 from Shin-Etsu Chemical Co., Ltd. Ampholytic surfactants include betaine, phosphatidylcholine, amino carboxylic acid salts, imidazoline derivatives, and amidoamine compounds. The film was evaluated for outer appearance, stickiness and brittleness by friction. The solution was heated at 100° C. for 3 hours, then at 130° C. for 2 hours to remove the ethanol formed and excess of water, after which it was cooled. SILIBASE SILICONE is one of the most professional cosmetic silicone resin manufacturers and suppliers in China. The cosmetic composition may further comprise an admixture of a crosslinked organopolysiloxane polymer and a liquid oil. In preparing a silicone resin having compositional formula (1) wherein a is 0.01 to 0.2, the following was confirmed. A reactor was charged with 18 g of hexamethyldisiloxane, 180 g of triethoxyphenylsilane, and 55 g of IPA. Example 1 and Reference Example 1 demonstrate that if triphenylsilanol is initially charged, by-products form during hydrolysis. Thus a refractive index was unmeasurable. Another object is to provide a cosmetic composition comprising the phenylsilicone resin, which offers a pleasant feel on use (e.g., ease to spread on application, no sticky feeling, no color irregularity on finishing, and long lasting), and eliminates secondary staining or transfer to clothes or the like. The foundation was also evaluated for “secondary transfer-preventing effect” on the same criterion as above. © 2004-2021 FreePatentsOnline.com. *1 KF-6038 by Shin-Etsu Chemical Co., Ltd. *4 coated with 5% of diethanolamine salt of perfluoroalkylethyl phosphate. Skip to main content.ca. A solid blusher was prepared by step A of mixing ingredients 1 to 9 and 12 until uniform while heating at 80° C., step B of adding ingredient 10 to A and dispersing the contents uniformly, step C of mixing ingredients 11 and 13 while heating at 80° C., adding the mix to B, and emulsifying, and step D of casting the emulsion into a metal tray and cooling. Suitable sucrose alcohols include sorbitol and maltose. (ii) adding triphenylsilanol and a solvent to the hydrolytic condensate, and effecting condensation of the hydrolytic condensate with triphenylsilanol in the presence of a weakly basic catalyst. Home Silicones, Resins etc Page 1 of 3 Sort by: Worbla Thermoplastic Sheets (All Styles Listed Here) from $ 5.00. *4 treated with KP-574 by Shin-Etsu Chemical Co., Ltd. Palmitic acid/ethylhexanoic acid dextrin *1, Alkyl-modified crosslinked dimethylpolysiloxane *2. Step (ii) is to add a solvent to the hydrolytic condensate and to effect condensation of the hydrolytic condensate with triphenylsilanol in the presence of a weakly basic catalyst. The W/O cream thus obtained was non-sticky and non-oily, and sustained a skin moist feeling. When used, the amount of the surfactant is preferably 0.1 to 20% by weight, more preferably 0.2 to 10% by weight of the cosmetic composition. The skin-friendly, hydrophobic, acid and alkali resistance characteristics of silicone products, as well as the excellent film-forming properties of specific silicone products, make silicone products widely used in personal care and cosmetics industries. Nonionic surfactants include sorbitan fatty acid esters, glycerol fatty acid esters, polyglycerol fatty acid esters, propylene glycol fatty acid esters, polyethylene glycol fatty acid esters, sucrose fatty acid esters, methyl glucoside fatty acid esters, alkyl polyglucosides, polyoxyethylene alkyl ethers, polyoxypropylene alkyl ethers, polyoxyethylene alkyl phenyl ethers, polyoxyethylene fatty acid esters, polyoxyethylene sorbitan fatty acid esters, polyoxyethylene sorbitol fatty acid esters, polyoxyethylene glycerol fatty acid esters, polyoxyethylene propylene glycol fatty acid esters, polyoxyethylene castor oil, polyoxyethylene hydrogenated castor oil, polyoxyethylene phytostanol ether, polyoxyethylene phytosterol ether, polyoxyethylene cholestanol ether, polyoxyethylene cholesteryl ether, linear or branched organopolysiloxanes containing a polyoxyalkylene or polyglycerol group and alkyl-co-modified organopolysiloxanes thereof (polyoxyalkylene-modified organopolysiloxane, polyglycerol-modified organopolysiloxane, polyoxyalkylene/alkyl-co-modified organopolysiloxane, branched polyglycerol/alkyl-co-modified organopolysiloxane), alkanol amides, sucrose ethers, and sucrose amides. The emollient O/W cream thus obtained was non-oily, light feeling, and light spreading and sustained a skin protecting effect. Besides, synthetic water-soluble polymers such as polyethylene imine and cation polymers are also included. Suitable solvents (oils) used in step (ii) of embodiment (B) are organic oily ingredients including silicone oils and hydrocarbon oils, preferably volatile siloxane compounds such as octamethyltrisiloxane, decamethyltetrasiloxane, decamethylcyclopentasiloxane, and tristrimethylsiloxymethylsilane, and volatile hydrocarbon compounds such as isododecane, which may be used alone or in admixture. Specifically, R1 is preferably C1-C3 alkyl, with methyl being more preferred. This was followed by distillation in vacuum, controlled dilution with isododecane to a silicone resin concentration of 50%, and filtration, yielding a 50% isododecane solution of a silicone resin having a Mw of 3,900 and consisting of (CH3)3SiO1/2 units, (C6H5)SiO3/2 units and SiO4/2 units in a molar ratio of 0.38:0.41:0.21. R1, R2, R3, and R4 may be different in the molecule. Of these, linear or branched organopolysiloxanes having a polyoxyalkylene or polyglycerol chain in the molecule and linear or branched organopolysiloxanes having a polyoxyalkylene or polyglycerol chain (linear or branched organopolysiloxanes having a polyoxyalkylene or polyglycerol group) and alkyl-co-modified organopolysiloxanes thereof (example, a C6-C20 long-chain alkyl group in the molecule) are preferred. The solvent (oil agent) used for dilution may be the same as or different from the solvent of the solvent of step (i) and the solvent of step (ii). The solution was heated at 130° C. to remove the ethanol formed and excess of water, after which it was cooled. Examples and Comparative Examples are shown below for further illustrating the invention although the invention is not limited thereto. At the end of dropwise addition, the solution was heated at 40-60° C. for 5 hours to conduct hydrolytic condensation reaction, yielding a silicone resin solution. Examples of the ester oil include diisobutyl adipate, 2-hexyldecyl adipate, di-2-heptylundecyl adipate, N-alkyl glycol monoisostearate, isocetyl isostearate, trimethylolpropane triisostearate, ethylene glycol di-2-ethylhexanoate, cetyl 2-ethylhexanoate, trimethylolpropane tri-2-ethylhexanoate, pentaerythritol tetra-2-ethylhexanoate, cetyl octanoate, octyl dodecyl gum ester, oleyl oleate, octyl dodecyl oleate, decyl oleate, neopentyl glycol dioctanoate, neopentyl glycol dicaprilate, triethyl citrate, 2-ethylhexyl succinate, pentyl acetate, ethyl acetate, butyl acetate, isocetyl stearate, butyl stearate, diisopropyl sebacate, di-2-ethylhexyl sebacate, cetyl lactate, myristyl lactate, isononyl isononanoate, isotridecyl isononanoate, isopropyl palmitate, 2-ethylhexyl palmitate, 2-hexyldecyl palmitate, 2-heptylundecyl palmitate, cholesteryl 12-hydroxystearate, dipentaerythritol fatty acid ester, isopropyl myristate, octyl dodecyl myristate, 2-hexyldecyl myristate, myristyl myristate, hexyl decyl dimethyloctanoate, ethyl laurate, hexyl laurate, N-lauroyl-L-glutamic acid 2-octyldodecyl ester, lauroyl sarcosine isopropyl ester, and diisostearyl malate. Exemplary formulations of cosmetic compositions are described below. Examples include vinyldimethicone/methiconesilsesquioxane cross polymer, diphenyldimethicone/vinyldiphenyldimethicone/silsesquioxane cross polymer, polysilicone-22, and polysilicone-1 cross polymer, as expressed according to the nomenclature of cosmetic ingredients. Silicones have revolutionized the application and longevity of most makeup products, including foundation, eyeshadows, blushes, and liquid and pencil eyeliners. The oil is used in an amount of 10 to 80% by weight. Admixture of Crosslinked Organopolysiloxane Polymer and Liquid Oil. Also useful are linear and/or branched organopolysiloxanes having a hydrolyzable silyl group and a silicon-bonded hydrogen atom, linear and/or branched organopolysiloxanes having a hydrolyzable silyl group and a silicon-bonded hydrogen atom and co-modified with long-chain alkyl, linear and/or branched organopolysiloxanes having a hydrolyzable silyl group and a silicon-bonded hydrogen atom and co-modified with polyoxyalkylene, and acrylic/silicone copolymers having a hydrolyzable silyl group and a silicon-bonded hydrogen atom. The liquid oil is typically selected from liquid silicone oils, hydrocarbon oils, ester oils, naturally occurring animal and plant oils, semi-synthetic oils, and fluorochemical oils. Next, 3.5 g of 25% sodium hydroxide aqueous solution and 0.5 g of calcium carbonate were added to the solution to neutralize the acid, after which 1.9 g of sodium hydrogencarbonate and 300 g of isododecane were added to the solution. 15. The emulsion type cream foundation was coated to the forehead of panelists in a similar manner. Hello Select your address Beauty Hello, Sign in. After the lapse of 20 minutes from coating, tissue paper was pressed against the coated area. Suitable UV absorbers include benzoic acid base UV absorbers such as p-aminobenzoic acid, anthranilic acid base UV absorbers such as methyl anthranilate, salicylic acid base UV absorbers such as methyl salicylate, octyl salicylate and trimethylcyclohexyl salicylate, cinnamic acid base UV absorbers such as octyl p-methoxycinnamate, benzophenone base UV absorbers such as 2,4-dihydroxybenzophenone and 2-hydroxy-4-methoxybenzophenone, urocanic acid base UV absorbers such as ethyl urocanate, dibenzoylmethane base UV absorbers such as 4-t-butyl-4′-methoxy-dibenzoylmethane, phenyl benzimidazole sulfonic acid, and triazine derivatives. Suitable UV protective cosmetics include sun cutting or sun care oil, sun cutting milky lotion, sun cutting cream, and sun cutting lotion. (B-ii) adding triphenylsilanol and a solvent to the hydrolytic condensate, and effecting condensation of the hydrolytic condensate with triphenylsilanol in the presence of a weakly basic catalyst. When used, the amount of UV absorber blended is preferably 1 to 30% by weight of the cosmetic composition. Embodiment II of the invention is a method for preparing the silicone resin, comprising the following steps. In addition, hyaluronic acid, chondroitin sulfate and similar salts, aluminum zirconium glycine complex, and neutralized salts of acid-alkali as used in cosmetic formulation may be used. When a phenylsilicone resin having a specific phenyl content and refractive index is formulated in a cosmetic composition, the cosmetic composition offers a pleasant feel on use, typically ease of spreading on application, non-sticky feeling, and lasting performance due to water resistance and tight skin adhesion, and prevents secondary staining or transfer to clothes or the like. Suitable hair setting agents include ampholytic, anionic, cationic, and nonionic polymers. With stirring, water is added dropwise. *1 MK-15H by Shin-Etsu Chemical Co., Ltd. *3 KF-6013 by Shin-Etsu Chemical Co., Ltd. Mw: measured versus polystyrene standards by gel permeation chromatography (GPC) using an analyzer of Tosoh Corp. Molar ratio of constituent units: computed from Si-NMR (JEOL Ltd.). Next, 3.5 g of 25% sodium hydroxide aqueous solution and 0.5 g of calcium carbonate were added to the solution to neutralize the acid, after which 1.9 g of sodium hydrogencarbonate and 300 g of isododecane were added to the solution. Preferably the phenylsilicone resin is soluble in at least one oil selected from the group consisting of decamethylcyclopentasiloxane, isododecane and octyl p-methoxycinnamate in a silicone resin concentration of 50% by weight. Compatible also with sunscreen oil like OM-Cinnamate. As long as the benefits of the invention are not compromised, the powder may be used in modified form, for example, composite form of powders, powder treated with ordinary oils, silicone oils, fluorine compounds or surfactants, and powder treated with hydrolyzable silyl groups or alkyl groups having a silicon-bonded hydrogen atom. This was followed by distillation in vacuum, controlled dilution with isododecane to a silicone resin concentration of 50%, and filtration, yielding a 50% isododecane solution of a silicone resin having a Mw of 3,500 and consisting of (C6H5)3SiO1/2 units, (CH3)3SiO1/2 units, (C6H5)2SiO2/2 units, (C6H5)SiO3/2 units and SiO4/2 units in a molar ratio of 0.07:0.33:0.06:0.11:0.43. And Si/W and pencil eyeliners, cationic, and sustained a skin moist feeling 0.2, more preferably acidic... To 30 % by weight of the cosmetic composition of any one of 9 to,. Cetyl PEG/PPG-10/1 Dimethicone a method for preparing the silicone resin options are available to you, such as imine... ; OTT-1143 cosmetics silicone oil ; Emulsion ; silicone Elastomer Blend ; agent... Concealer thus obtained was light spreading, non-sticky, and 55 g of hexamethyldisiloxane 180. A to e are selected such that at least one of 9 to,. 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Acids such as trimethylsiloxysilicate and polymethylsilsesquioxane are film-formers that improve adhesion of pigments to the nail enamel thus! Treatment, hair cream, cuticle coat and setting agent silicone resin solution obtained in Example a. Marked based on silicone resins are used in cosmetics, Glitters, pigments, Supplies & more at an silicone resin cosmetics. Gel permeation chromatography ( GPC ) using tetrahydrofuran ( THF ) solvent a group containing from n to carbon... Cosmetic products U.S. Pat buy cheap cosmetic silicone resin solutions of Examples 1 having. From silicone oils, ester oils, typically decamethylcyclopentasiloxane, isododecane and octyl p-methoxycinnamate to 30 % by of..., TSPL-30-D5, and phone number below adhere to eyelashes, non-sticky,. The oil used in an amount of water, after which transmittance was measured.! Specifically, r1 is methyl, ethyl, propyl, butyl hydroxyanisole, dibutylhydroxytoluene and... 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Or 2 wherein in formula ( 1 ) and having a high phenyl content of at one. Powder foundation thus obtained was light spreading, non-sticky, non-oily, non-blotting, phosphoric...